Sunday, March 09, 2014 9:11:17 PM Beaver Bong
00 grams (100 ml) of hydrazine hydrate is mixed with 140 grams
powdered sodium hydroxide. The apparatus is thoroughly flushed
with nitrogen, then the rate of nitrogen addition to the distilling flask
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is slowed, and fractional distillation is commenced through an
efficient fractionating column of about 15 theoretical plates.
Anhydrous hydrazine distills at 112° C to 114° C. Anhydrous
hydrazine is obtained at 99%+ purity.
Another method for producing anhydrous hydrazine exists which
gives a higher yield of product, but it uses anhydrous ammonia and
more complicated glassware and procedures. See Journal of the
American Chemical Society Volume 73, page 1619 (1951), and
Volume 76, page 3914 (1954). Also see Hydrazine by C.C. Clark, The
Chemistry of Hydrazine by L.F. Audrieth, and Industrial and
Engineering Chemistry Volume 45, pages 2608 and 2612 (1953).
Also see Inorganic Syntheses Volume 1, page 90 (1939).
Anhydrous hydrazine can be stored in dark glass bottles under
refrigeration for years.
Other variations on the alkali hydroxide dehydration of hydrazine
hydrate exist which give higher yields of less-pure hydrazine. See
pages 48-54 in the Chemistry of Hydrazine mentioned above. It lists
many references. Especially interesting is Journal of the American
Chemical Society Volume 71, pages 1644-47 (1949).
Preparation of Diethvlamine
NH3 + CH3CH2I —s> xHI + CH3CH2NH2
+ (CH3CH2)2NH +
(CH3CH2 ) 3N
The reaction which produces diethylamine also yields as byproducts
ethylamine and triethylamine. The relative amounts of each
compound produced depends upon the molar ratio of the two starting
materials. Use of only a little ethyl iodide favors the formation of
mostly ethylamine. Use of a lot of the ethyl iodide favors the
formation of triethylamine. Somewhere in the middle, a roughly even
split occurs. This will be done here. See Journal of the American
Chemical Society Volume 69, pages 836 to 838 (1947).
LSD Directly From The Lysergic Amides —
The One Pot Shot 37
A section of clean steel pipe 2l/2 to 3 inches in diameter is
obtained, and fine threads are cut into each end so that a cap may be
screwed onto each end. A really nice touch would be to have all the
pieces plated with a half-thousandths-inch of electroless nickel, but
the plater may think you are constructing a pipe bomb when he sees
the pipe and caps.
The bottom of the pipe is secured by screwing the cap on over
threads coated with Teflon tape. Welding may also be used. The pipe is
then nestled into a Styrofoam cooler, and is then filled about Vi full of
rubbing alcohol, and then to this solvent dry ice is added, slowly at first
to prevent it from boiling over, then more rapidly. The top of the pipe
should be covered to prevent frost from forming inside the pipe as it
Next, add 175 ml of ethyl iodide to the pipe, and let it cool down. It
will not freeze, as its melting point is about 100° below O° C. The
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